Pharmaceutical

4-NITROBENZHYDRAZIDE

  • CAS:636-97-5
  • purity:99%
Inquiry

Manufacturer supply high quality 4-NITROBENZHYDRAZIDE 636-97-5 with GMP standards

  • Molecular Formula: C7H7 N3 O3
  • Molecular Weight: 181.151
  • Appearance/Colour: yellow crystalline powder 
  • Melting Point: 210-214 °C 
  • Refractive Index: 1.5860 (estimate) 
  • Boiling Point: 292.97°C (rough estimate) 
  • PKA: 2.77, 11.17(at 25℃) 
  • PSA: 100.94000 
  • Density: 1.406 g/cm3 
  • LogP: 1.81270 

4-NITROBENZHYDRAZIDE(Cas 636-97-5) Usage

Synthesis

Dissolve 218 g of p-nitrobenzyl acetate in 500 ml of hot methanol, stir, and slowly add 380 g of 15% sodium hydroxide solution. After the addition was completed, it was placed for 5 minutes, and then poured into ice water to precipitate a precipitate. The filtered precipitate was decolorized with activated carbon in hot water, and recrystallized to give?p-nitrobenzoicacidhydrazide 110-121 g .

Definition

ChEBI: A C-nitro compound in which the nitro group is substituted into the 4-position of benzohydrazide.

InChI:InChI=1/C7H7N3O3/c8-9-7(11)5-1-3-6(4-2-5)10(12)13/h1-4H,8H2,(H,9,11)

636-97-5 Relevant articles

Visual and near IR (NIR) fluorescence detection of Cr3+ in aqueous media via spirobenzopyran ring opening with application in logic gate and bio-imaging

Goswami, Shyamaprosad,Das, Avijit Kumar,Maity, Anup Kumar,Manna, Abhishek,Aich, Krishnendu,Maity, Sibaprasad,Saha, Partha,Mandal, Tarun Kanti

, p. 231 - 239 (2014)

A new spirobenzopyran derivative (SPNH) ...

A new Pd(II)-Hydrazide-Triphenylphosphine complex: Synthesis, crystal structure, spectroscopic characterization and theoretical calculations

ünver, Hakan,Dikmen, G?khan

, (2021)

A new palladium(II) complex, [Pd(PPh3)(4...

A simple naphthalene-based colorimetric sensor selective for acetate

Goswami, Shyamaprosad,Das, Avijit Kumar,Sen, Debabrata,Aich, Krishnendu,Fun, Hoong-Kun,Quah, Ching Kheng

, p. 4819 - 4823 (2012)

A new naphthalene based receptor (L) has...

Synthesis, spectroscopic and structural evaluation of ethyl 2-cyano-3-{5-[(4-nitro-benzoyl)-hydrazonomethyl]-1H-pyrrol-2-yl}-acrylate using experimental and theoretical approaches

Singh,Kumar, Amit,Rawat, Poonam,Srivastsva, Anchal

, p. 419 - 428 (2013)

A new C-vinylpyrrole containing aroylhyd...

Design, Synthesis, and Study of the Insecticidal Activity of Novel Steroidal 1,3,4-Oxadiazoles

Bai, Hangyu,Jiang, Weiqi,Li, Qi,Li, Tian,Ma, Shichuang,Shi, Baojun,Wu, Wenjun

, p. 11572 - 11581 (2021/10/12)

A series of novel steroidal derivatives ...

Design and synthesis of novel 1,3,4-oxadiazole based azaspirocycles catalyzed by NaI under mild condition and evaluated their antidiabetic and antibacterial activities

Radia, Ashish J.,Lalpara, Jaydeep N.,Modasiya, Ishita J.,Dubal, Gaurang G.

, p. 612 - 621 (2020/12/14)

A modest, efficient, and mild synthetic ...

Synthesis, characterization, and biological evaluation of new derivatives targeting MbtI as antitubercular agents

Mori, Matteo,Stelitano, Giovanni,Chiarelli, Laurent R.,Cazzaniga, Giulia,Gelain, Arianna,Barlocco, Daniela,Pini, Elena,Meneghetti, Fiorella,Villa, Stefania

, p. 1 - 17 (2021/02/26)

Tuberculosis (TB) causes millions of dea...

636-97-5 Process route

4-nitrophenyl 4-nitrobenzoate
1037-31-6

4-nitrophenyl 4-nitrobenzoate

4-nitro-phenol
100-02-7,78813-13-5,89830-32-0

4-nitro-phenol

N-amino-(4-nitrophenyl)carboxamide
636-97-5

N-amino-(4-nitrophenyl)carboxamide

Conditions
Conditions Yield
With hydrazine; In water; dimethyl sulfoxide; at 25 ℃; Rate constant;
hydrazine hydrate
7803-57-8,79785-97-0

hydrazine hydrate

4-nitro-benzoic acid
62-23-7

4-nitro-benzoic acid

N-amino-(4-nitrophenyl)carboxamide
636-97-5

N-amino-(4-nitrophenyl)carboxamide

Conditions
Conditions Yield
With sulfuric acid; In ethanol; for 9h; Reflux;
66%

636-97-5 Upstream products

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    4-nitrophenyl 4-nitrobenzoate

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    4-nitro-benzoyl chloride

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